Poly(furfuryl alcohol) was prepared using methylene dichloride as solvent a
nd trifluoroacetic acid as catalyst. Synthesis was monitored in order to ac
hieve a desirable structure capable of crosslinking under the action of lig
ht. The resulting product was a soluble dark brown resin that gave remarkab
le photocrosslinking performance as a negative photoresist when exposed to
ultraviolet light, giving photolithographic patterns with a resolution of a
bout 5 mu m. (C) 1999 Elsevier Science Ltd. All rights reserved.