Si. Lee et al., Interfacial properties of glass fiber brittle-ductile dual-matrix composites using micromechanical techniques and acoustic emission, POLYM COMP, 20(1), 1999, pp. 19-28
The interfacial adhesion and microfailure modes of glass fiber-reinforced b
rittle unsaturated polyester/modified epoxy composites were investigated vi
a micromechanical techniques and acoustic emission (AE). Various silane cou
pling agents caused different degrees of interfacial adhesion and subsequen
t microfailure modes. In the brittle matrix layer, the number of matrix fra
gments was significantly influenced by the type of silane coupling agents.
The more cracks, the higher the interfacial adhesion under both dry and wet
conditions. This is attributed to the chemical and hydrogen bondings in tw
o interphases. The results obtained from microdroplet and fragmentation tes
ts were correlated by associating with the AE technique. The sequential occ
urrence of mainly three groups of AE were as follows: the first group origi
nated mainly from brittle matrix cracking. The second and the third groups
resulted in fiber breakage and ductile matrix cracking and debonding. For d
ual-matrix specimens the micromechanical tests provide reliable information
with regard to the interfacial adhesion and characterize the microfailure
modes when combined with the AE technique.