There are presented studies on the synthesis of aryl hydrazones of omega-ph
enylsulfonyl-acetophenone in reaction of phenacyl-phenyl sulphone with diaz
onium compounds carried out at alkaline medium. Elemental analysis UV and I
R spectroscopy confirmed the structure of synthesized compounds. Calculatio
ns proved the occurrence of the hydrogen bond between oxygen of sulfonyl gr
oup and hydrogen of hydrazone group. Some of synthesized compounds show pho
todynamic action.