Complete H-1 and C-13 NMR spectral assignment of 6,7,8,9-tetrahydro-7,7-dimethyldioxolo [5,4-b]acridin-9-one using FUCOUP

Authors
Nascimento, CJ Cruz, ER Figueroa-Villar, JD
Citation
Cj. Nascimento et al., Complete H-1 and C-13 NMR spectral assignment of 6,7,8,9-tetrahydro-7,7-dimethyldioxolo [5,4-b]acridin-9-one using FUCOUP, MAGN RES CH, 37(3), 1999, pp. 239-242
Citations number
8
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MAGNETIC RESONANCE IN CHEMISTRY
ISSN journal
07491581 → ACNP
Volume
37
Issue
3
Year of publication
1999
Pages
239 - 242
Database
ISI
SICI code
0749-1581(199903)37:3<239:CHACNS>2.0.ZU;2-M
Abstract
Unambiguous H-1 and C-13 chemical shift assignments of the novel antibiotic 6,7,8,9-tetrahydro-7,7-dimethyl-dioxolo[5,4-b]acridin-9-one were made usin g the FUCOUP pulse sequence. The appropriate phase cycling was calculated u sing the Compact Cartesian Coordinate Product Operator (C3PO) method. Copyr ight (C) 1999 John Wiley & Sons, Ltd.