Wide-angle X-ray scattering (WAXRS) in the 0.5-2.5 Angstrom(-1) region of t
he intensity curve of Beulah Zap (BZ) lignite indicates that the average di
stance between adjacent layers is ca. 3.5 Angstrom. The resulting interlaye
r structural curve, calculated by Fourier transform from the WAXRS intensit
y, indicates that only two layers occur in the average short-range structur
al domain of BZ with the distances between atoms in the adjacent layers occ
urring between 3.4 and 5.7 Angstrom. Both the WAXRS intensity curve (in rec
iprocal space) and the interlayer structure curve (in molecular space) are
consistent with an average short-range structural domain in which the flexi
ble spacers (attachments) between the polycyclic units are important contri
butors and where the PC units in the adjacent chains are not eclipsed.