F. Meschke et al., FAILURE BEHAVIOR OF ALUMINA AND ALUMINA SILICON-CARBIDE NANOCOMPOSITES WITH NATURAL AND ARTIFICIAL FLAWS, Journal of materials research, 12(12), 1997, pp. 3307-3315
Alumina/silicon carbide nanocomposites with 5 vol. % SiC nanoparticles
were produced by slip casting, pressureless sintering, and hot isosta
tic pressing. The grain size dependence of both the bend strength and
fracture toughness have been investigated. The strength exceeds 1 GPa
at a grain size of 1.7 mu m. Crack opening displacements (GOD) were me
asured, revealing that crack tip toughness is considerably lower than
in pure alumina and an R-curve behavior is unlikely to occur. By intro
ducing artificial pores with a size of 60 mu m, the micromechanical fr
acture process has been studied in both pure alumina and nanocomposite
s. In contrast to alumina, where an annular precrack forms prior to fr
acture, it is suggested that precrack formation is strongly impeded in
the nanocomposites and failure is controlled by microcrack initiation
. The high strength of Al2O3/SiC nanocomposites seems to be the result
of an unusually high crack initiation stress.