Hm. Hawthorne et al., THE MICROSTRUCTURAL DEPENDENCE OF WEAR AND INDENTATION BEHAVIOR OF SOME PLASMA-SPRAYED ALUMINA COATINGS, Wear, 203, 1997, pp. 709-714
Plasma-sprayed coatings are built up from individual overlapping solid
ified droplets, and the nature of boundaries between these ''splats''
influences their mechanical and wear characteristics. This work aims t
o elucidate the correlation between these characteristics and microstr
uctural features of model coatings produced under well-controlled proc
essing conditions. A series of coatings with different average splat s
ize were sprayed from pure alumina powders of different particle size
using an axial-injection plasma-spray torch under conditions optimized
to obtain the best microstructures. Phase composition was determined
by X-ray diffraction, while SEM with image analysis of polished and fr
actured surfaces was used to evaluate coating microstructures, and ind
entation and wear damage. Coatings were characterized by depth-sensing
indentation (DSI) at the sub-splat scale and by DSI, micro- and macro
-indentation at multiple splat scales. Both abrasion and dry-particle
erosion behaviour of the coatings were also investigated. Results reve
al the role of microstructural features on the material performance, p
articularly the critical influence of porosity, splat (grain) size and
inter-splat cohesion, on the multiple-splat scale wear and indentatio
n behaviour of the coatings. (C) 1997 Elsevier Science S.A.