Y. Takigawa et al., SUPERPLASTICITY IN AL2O3-20VOL-PERCENT SPINEL (MGO-CENTER-DOT-1-CENTER-DOT-5AL(2)O(3)) CERAMICS, Ceramics international, 24(1), 1998, pp. 61-66
Superplasticity in Al2O3-20 vol% spinel (MgO.1.5Al(2)O(3)) is investig
ated by means of tensile testing in the temperature range 1300-1550 de
grees C. The dispersion of spinel phase in Al2O3 slightly reduces the
flow stress, and highly enhances the high-temperature ductility at the
same stress level in comparison with 0.1 wt% MgO-doped single-phase A
l2O3. A maximum elongation of 396% is obtained at 1550 degrees C and a
strain rate of 24x10(-4)s(-1). The flow stress reduction is associate
d with a slight reduction in activation energy for superplastic flow.
The extensive ductility in Al2O3-20 vol% spinel cannot be explained on
ly from the stress reduction. The Al2O3/spinel boundaries are expected
to have much larger resistance to crack extension than Al2O3 grain bo
undaries. (C) 1997 Elsevier Science Limited and Techna S.r.l.