DETERMINATION OF THE REGIOSELECTIVITY AND ENANTIOSELECTIVITY OF THE ENZYMATIC HYDROLYZES OF SUCCINATES BASED ON H,C COLOC ANALYSIS AND DEUTERIUM NMR IN A CHIRAL LIQUID-CRYSTAL

Authors
CHEVTCHOUK T OLLIVIER J SALAUN J MERLET D COURTIEU J
Citation
T. Chevtchouk et al., DETERMINATION OF THE REGIOSELECTIVITY AND ENANTIOSELECTIVITY OF THE ENZYMATIC HYDROLYZES OF SUCCINATES BASED ON H,C COLOC ANALYSIS AND DEUTERIUM NMR IN A CHIRAL LIQUID-CRYSTAL, Tetrahedron : asymmetry, 8(7), 1997, pp. 999-1003
Citations number
25
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear","Chemistry Physical
Journal title
Tetrahedron : asymmetry → ACNP
ISSN journal
09574166
Volume
8
Issue
7
Year of publication
1997
Pages
999 - 1003
Database
ISI
SICI code
0957-4166(1997)8:7<999:DOTRAE>2.0.ZU;2-M
Abstract
The regio- and enantiomeric excess analyses of (S)-half esters resulti ng from enzymatic (lipase, esterase) hydrolyses of chiral dimethyl suc cinates, were accurately determined from H,C COLOC experiments and H-2 NMR in liquid crystal (PBLG, CH2Cl2). (C) 1997 Elsevier Science Ltd.