SYNTHESIS AND HYDROLYSIS OF HYBRIDIZED SILICON ALKOXIDE - SI(OET)(X)(OBUT)(4-X) .2. HYDROLYSIS OF THE SI(OET)(X)(OBUT)(4-X)

Authors
CAO B ZHANG Z ZHU CS
Citation
B. Cao et al., SYNTHESIS AND HYDROLYSIS OF HYBRIDIZED SILICON ALKOXIDE - SI(OET)(X)(OBUT)(4-X) .2. HYDROLYSIS OF THE SI(OET)(X)(OBUT)(4-X), JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 10(3), 1997, pp. 255-261
Citations number
14
Journal title
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY → ACNP
ISSN journal
09280707
Volume
10
Issue
3
Year of publication
1997
Pages
255 - 261
Database
ISI
SICI code
0928-0707(1997)10:3<255:SAHOHS>2.0.ZU;2-Y
Abstract
The hydrolyzation behavior of the Si(OEt)(x)(OBut)(4-x) synthesized in part I was investigated by gas chromatogram/mass spectrum (GC/MS) tec hnique. In the Si(OEt)(x)(OBut)(4-x), Si(OEt)(OBut)(3) showed more rap id hydrolysis than Si(OEt)(2)(OBut)(2), especially in the initial stag es of the hydrolyzation. The dimer and trimer formations along with th e sol-gel course were followed during the hydrolyzation process.