F. Sanchette et al., SINGLE-CYCLE PLASMA NITRIDING AND HARD COATING DEPOSITION IN A CATHODIC ARC EVAPORATION DEVICE, Surface & coatings technology, 94-5(1-3), 1997, pp. 261-267
The duplex treatment of alloy steel (nitriding + hard coating) has bee
n studied for a few years now. It is an interesting method not only fo
r increasing fatigue strength and tempering resistance bur also for im
proving corrosion and wear behaviours, particularly under high loads.
Such treatments are used for dieing or hot-working applications and ar
e often performed with a discontinuous combination of nitriding and ha
rd coating. This solution has some disadvantages with regards to inter
mediate external steps prior to coating/polishing and grinding. The ai
m of this work is to investigate the possibilities and interests of pe
rforming duplex treatment during a single cycle within an industrial c
athodic are evaporation PVD device. Two types of plasma nitriding were
tested: 'conventional' plasma nitriding in N-2 + H-2 mixtures and low
-pressure enhanced plasma nitriding assisted by an electron beam produ
ced by a new are evaporation source. Hard coatings (TiN or CrN) with g
ood adhesion can be deposited on nitrided high-alloy steels if nitridi
ng, ion cleaning and coating parameters are adjusted. A smooth surface
on the bright nitrided substrate (without compound layer) prior to th
e coating stage must be achieved in order to reach the best mechanical
properties of the composite. This technology, which does not require
additional polishing steps before completion, can result not only in l
ower production costs but in high continuity between the two stages of
duplex treatment. (C) 1997 Elsevier Science S.A.