M. Faryna et al., SEM STUDIES OF MICROSTRUCTURAL DEVELOPMENT DURING SINTERING OF TI3SIC2-BASED COMPOSITES, Journal of trace and microprobe techniques, 15(4), 1997, pp. 453-457
A densification of the bulk material obtained from powders prepared by
a combustion technique using pressureless sintering occurs with some
secondary phenomena such as liquid-phase reactions with transient inte
rmetallic phase and recrystalization of grains. As a result, the mater
ial with controlled microstructure in form of particulate composites,
consisting of Ti3SiC2 matrix and TiC inclusions, can be obtained. This
paper reports SEM and EDS studies of microstructure development durin
g sintering.