HYDROTHERMAL SYNTHESIS AND CHARACTERIZATI ON OF A NOVEL LOW-TEMPERATURE PHASE K3SB0.3Y4O8-CENTER-DOT-6H(2)O

Authors
ZHENG WJ XU YH PANG WQ
Citation
Wj. Zheng et al., HYDROTHERMAL SYNTHESIS AND CHARACTERIZATI ON OF A NOVEL LOW-TEMPERATURE PHASE K3SB0.3Y4O8-CENTER-DOT-6H(2)O, Gaodeng xuexiao huaxue xuebao, 18(12), 1997, pp. 1932-1934
Citations number
6
Journal title
Gaodeng xuexiao huaxue xuebao → ACNP
ISSN journal
02510790
Volume
18
Issue
12
Year of publication
1997
Pages
1932 - 1934
Database
ISI
SICI code
0251-0790(1997)18:12<1932:HSACOO>2.0.ZU;2-6
Abstract
A novel low temperature phase K3Sb0.3Y4O8 . 6H(2)O was synthesized hyd rothermally from K2O-Sb2O3-Y2O3-H2O system, and characterized by means of XRD, SEM, IR, TG, DTA and ICP methods. The unit cell for the produ ct is hexagonal with the cell parameters a=1.657 6 nm and c=1.186 5 nm . The volume of the cell is calculated to be 2.823 3 nm(3). The produc t was decomposed into oxides from 310 degrees C to 390 degrees C.