E. Schonherr et al., IN-SITU OBSERVED TWIN FORMATION ON ZNSE CRYSTALS GROWING BY SUBLIMATION, Crystal research and technology, 32(8), 1997, pp. 1041-1047
ZnSe crystals were grown by sublimation in closed ampoules between 133
5 K and 1365 K. The growth was observed in situ with a video camera af
ter an abrupt change of the supersaturation. The crystals developed pr
eferably {110} faces. Repeatedly a nucleus was formed in ortho-twin po
sition on a small {111} face which truncated the corner of three adjac
ent {110} faces. The repeated twin formation led to a preferred growth
into the relevant <111> direction. The twinning already occurred at a
low supercooling of less than 1 K and accelerated the growth distinct
ly.