Jm. Alves et Am. Vallera, HIGH-TEMPERATURE SOUND-VELOCITY MEASUREMENT WITH PIEZOELECTRIC TRANSDUCERS, Review of scientific instruments, 69(1), 1998, pp. 130-132
A technique for high temperature sound velocity measurement using piez
oelectric transducers, that avoids the existence of the usual high tem
perature bond between the sample and the buffer, was developed. This b
ond is frequently responsible for a large attenuation and distortion o
f the sound field, with a consequent inaccuracy in the experimental re
sults. This technique was successfully used by the authors to make goo
d quality measurements of sound velocity in iron-silicon single crysta
ls from room temperature to T approximate to 1000 degrees C, unlike ot
her authors who report strong attenuation in different regions of this
temperature range for similar samples. The furnace, which is only 35
mm wide, allows work under magnetic held and a controlled atmosphere u
p to 1300 degrees C. (C) 1998 American Institute of Physics.