V-loaded beta zeolites can be prepared by a two-step postsynthesis met
hod which consists of first creating vacant T-sites by dealumination o
f the beta zeolite with nitric acid, then contacting them with an ammo
nium metavanadate solution; the SiOH consumption and the nature of the
incorporated V species are characterized by IR, W-VIS and Si-29 MAS N
MR spectroscopies.