SELF-ASSEMBLY OF N,O-BIS(TRIMETHYLSILYL) AMINO-ACIDS TO PEPTIDES MEDIATED BY O-PHENYLENE PHOSPHOROCHLORIDATE IDENTIFIED BY FAST-ATOM-BOMBARDMENT MASS-SPECTROMETRY
H. Fu et al., SELF-ASSEMBLY OF N,O-BIS(TRIMETHYLSILYL) AMINO-ACIDS TO PEPTIDES MEDIATED BY O-PHENYLENE PHOSPHOROCHLORIDATE IDENTIFIED BY FAST-ATOM-BOMBARDMENT MASS-SPECTROMETRY, Rapid communications in mass spectrometry, 12(2), 1998, pp. 94-96
The self assembly of N,O-bis(trimethylsilyl)amino acids to form peptid
es, mediated by o-phenylene phosphorochloridate, was investigated by p
ositive ion fast atom bombardment and B/E linked-scan techniques witho
ut isolation and purification prior to analysis. The expected results
were confirmed by considering the fragmentation regularity of peptides
. (C) 1998 John Wiley & Sons, Ltd.