SOLVENT VERSATILITY OF BONDED CELLULOSE-DERIVED CHIRAL STATIONARY PHASES FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND ITS CONSEQUENCES INCOLUMN LOADABILITY

Authors
FRANCO P MINGUILLON C OLIVEROS L
Citation
P. Franco et al., SOLVENT VERSATILITY OF BONDED CELLULOSE-DERIVED CHIRAL STATIONARY PHASES FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND ITS CONSEQUENCES INCOLUMN LOADABILITY, Journal of chromatography, 793(2), 1998, pp. 239-247
Citations number
17
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Journal of chromatography → ACNP
Volume
793
Issue
2
Year of publication
1998
Pages
239 - 247
Database
ISI
SICI code
Abstract
The chromatographic behaviour of a 10-undecenoate/3,5-dimethylphenylca rbamate of cellulose bonded on allylsilica gel is tested using four or ganic mobile-phase modifiers (2-propanol, chloroform, tetrahydrofuran and ethyl acetate). The advantages of the broad choice of solvents off ered by this kind of chiral stationary phases and their resistance are discussed. The loadability of the column and its dependence both on t he racemate to be resolved and on the solvent used as mobile phase are also discussed. (C) 1998 Elsevier Science B.V.