Structural analysis of metallic superlattices is essential for underst
anding their interesting transport properties like the giant magnetore
sistance (GMR) effect. We present a detailed analysis of the [Fe (4.8
Angstrom)/Cr (13 Angstrom)](50) superlattice which shows a record GMR
value. The analysis is done by simulating its x-ray diffraction spectr
um measured with a synchrotron x-ray source. The ingredients for this
simulation are obtained from simulations of x-ray diffraction spectra
of single Fe and Cr films. This way we reduce the number of free param
eters resulting in reliable values for the interfaces roughness. We al
so show that x-ray diffraction spectra of systems with low contrast in
electron density can be quantitatively analysed.