Jmk. Wiezorek et al., DETERMINING DIRECTLY FROM EXPERIMENT THE MAGNITUDE OF THE BURGERS VECTOR OF GLISSILE [C]-COMPONENT DISLOCATIONS IN TI3AL, Philosophical magazine letters, 75(5), 1997, pp. 281-289
The magnitude of the Burgers vector of glissile [c]-component dislocat
ions observed in polycrystalline alpha(2)-Ti3Al after room-temperature
compression has been determined directly and unambiguously using tran
smission electron microscopy. Previously only the direction of the Bur
gers vector of these types of defects has been determined unequivocall
y from experiment alone. The direct experimental determination of the
Burgers vector has been achieved by combining conventional diffraction
contrast experiments with a detailed analysis of the effects of these
[c]-component dislocations on thickness contours. Thus the defects re
sponsible for the limited accommodation of strains with components out
of the basal plane, c-component strains, during room-temperature defo
rmation have been identified to be pairs of [c+a/2] superpartial dislo
cations with Burgers vectors b = 1/6[(2) over bar 116] delineating a r
ibbon of antiphase boundary on second-order pyramidal planes, {(2) ove
r bar 11 (1) over bar}.