Vn. Pathak et al., SYNTHESIS AND SPECTRAL STUDIES OF SOME NOVEL -G]BENZO-8-ARYLPYRAZOLO[4,5-E][1,5-B]BENZOXAZONINE VIA PHASE-TRANSFER CATALYSIS, Synthetic communications, 27(10), 1997, pp. 1811-1818
Treatment of 1H-4,5-dihydro-3-aryl-5-(2-hydroxyaryl)pyrazole with o-di
bromoxylene under liquid-liquid phase transfer catalytic conditions us
ing tetra-n-butylammonium hydrogen sulphate or [18]crown-6 as PT catal
yst, benzene/chloroform as organic phase and 50% aqueous potassium hyd
roxide as second phase, afforded novel 2,5,9,10-tetrahydro [7,8-g] ben
zo-8-arylpyrazolo[4,5-e] [1,5-b] benzoxazonines.