C. Mathieu et al., IMAGING THE ATOMIC-SCALE STRUCTURE OF VANADIA POWDER SURFACE USING AMBIENT ATOMIC-FORCE MICROSCOPY, Surface science, 395(1), 1998, pp. 201-206
Constant force images of vanadia powder were recorded in ambient condi
tions with atomic force microscopy. Atomic-scale observations of the (
001) surface powder were obtained. The images reveal differences from
the ideal structure which are attributed to the presence of adsorbed m
olecular water. A diffuse reflectance infrared Fourier transform spect
roscopy study confirms this hypothesis and an adsorption model is prop
osed. (C) 1998 Elsevier Science B.V.