Jh. Jeong et D. Kwon, EVALUATION OF THE ADHESION STRENGTH IN DLC FILM-COATED SYSTEMS USING THE FILM-CRACKING TECHNIQUE, Journal of adhesion science and technology, 12(1), 1998, pp. 29-46
A theoretical analysis of the adhesion dependence of film-cracking beh
avior resulting from the uniaxial tensile loading of a hard film on a
ductile substrate is presented. An interface shear stress that develop
s due to the deformation mismatch of the film and substrate induces a
normal tensile stress in the film; these stresses are analyzed as a fu
nction of external strain and crack spacing, using the shear lag theor
y. When the film tensile stress exceeds the film fracture strength sig
ma(c), film cracking occurs at an early stage of uniaxial loading; but
as the loading increases, the interface shear stress increases above
the critical value tau(c) and causes the interface failure. After that
, no more film cracking occurs, since stress transfer into the film is
impossible due to interface damage. Thus, the interface adhesion can
be estimated in terms of the shear strength from the external strain e
psilon(sat) and crack spacing lambda(sat) measured at the time that fi
lm cracking stops. The test results for the diamond-like carbon (DLC)/
Al system show an increase of the interface shear strength by a factor
of 1.6 for 30-min Ar-plasma etching, compared with no etching. It was
found that as the etching time increased, epsilon(sat) increased and
lambda(sat) decreased, i.e. the interface shear strength increased. Th
is strong dependence of epsilon(sat) and lambda(sat) on interface adhe
sion indicates that these experimental parameters can be used as quali
tative measures of the interface adhesion in a given system.