Some typical temperature-programmed reduction (TPR) and hydrogen tempe
rature-programmed desorption (TPD) experiments on a 0.6%wt.Pt/Al2O3 ca
talyst have been analysed in conjunction with parallel ''in situ'' AC
electrical conductivity measurements, in order to gain more insight in
to the nature of the catalyst interaction with oxidizing and reducing
atmosphere. Comparative analysis of results demonstrates their similar
ity and indicates that ''in situ'' AC electrical measurements is a sui
table method for characterization of superficial properties of the cat
alysts.