Ls. Nadezhina et al., DETERMINATION OF PALLADIUM IN CHLORIDE SOLUTIONS BY STRIPPING VOLTAMMETRY AT A MERCURY GLASSY-CARBON ELECTRODE, Journal of analytical chemistry, 53(2), 1998, pp. 151-153
Specific features of the formation of mercury film coatings on glassy
carbon were studied in chloride solutions of different concentrations.
The deposition of a solid mercurous salt favored by H2O2 formed at th
e electrode occurs in aerated solutions. Two variants of a procedure f
or determining palladium were developed and then verified in real samp
les of spent palladium electrolytes.