A PRACTICAL SYNTHESIS OF N-P-ANISYL-N-METHYL-AMINO-3-(9-ANTHRYL)-PROPANE - AN EXCIPLEX FLUORESCENCE THERMOMETER

Authors
SPIVEY AC BISSELL AJ STAMMEN B
Citation
Ac. Spivey et al., A PRACTICAL SYNTHESIS OF N-P-ANISYL-N-METHYL-AMINO-3-(9-ANTHRYL)-PROPANE - AN EXCIPLEX FLUORESCENCE THERMOMETER, Synthetic communications, 28(4), 1998, pp. 623-632
Citations number
30
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Synthetic communications → ACNP
ISSN journal
00397911
Volume
28
Issue
4
Year of publication
1998
Pages
623 - 632
Database
ISI
SICI code
0039-7911(1998)28:4<623:APSON>2.0.ZU;2-T
Abstract
A practical synthesis of N-p-anisyl-N-methyl-amino-3-(9-anthryl)-propa ne from 9-anthraldehyde is described. All the intermediates in this si mple five step sequence are crystalline and simple recrystallisation a fter each step allows the preparation of this exciplex fluorescence 't hermometer' molecule on a preparative scale without resort to chromato graphy.