Cathodic stripping voltammetry was used to determine the antibacterial
drug Nitrofurantoin in phosphate buffer (pH 5.5). The adsorptive peak
was observed at -0.173 V vs. Ag/AgCl. The peak response was character
ized with respect to pH, preconcetration time, possible interferences,
deposition potential, supporting electrolytes and other variables. Th
e obtained results were analyzed and the statistical parameters were c
alculated Also the method was applied to determine the mentioned lug i
n pharmaceutical formulations and urine. The limit of detection was 1x
10(-9) mol dm(-3).