ALKACYMETRIC AGENTS APPLICATION TO PHENOLS VISUALIZING IN THIN-LAYER CHROMATOGRAPHY

Citation
W. Wardas et al., ALKACYMETRIC AGENTS APPLICATION TO PHENOLS VISUALIZING IN THIN-LAYER CHROMATOGRAPHY, Chemia Analityczna, 43(1), 1998, pp. 99-106
Citations number
17
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00092223
Volume
43
Issue
1
Year of publication
1998
Pages
99 - 106
Database
ISI
SICI code
0009-2223(1998)43:1<99:AAATPV>2.0.ZU;2-E
Abstract
10 new visualising agents, among which 8 were alkacymetric indicators, were applied for visualising some monohydroxyphenols. Visualising eff ects for the phenols were investigated on silica gel on a mixture of s ilica gel and kieselguhr and on polyamide. Most of the investigated ph enols were detected on silica gel, and less on polyamide. The best det ectability (from 20 to 100 ng) was obtained for p-nitrophenol (after s eparation on adsorbents A, B, and C), alpha-naphtol (sorbents A and B) , and beta-naphtol (sorbent B). The best and most universal visualisin g agents for the investigated phenols were bromocresol green, bromothy mol blue, and known as redoxymetric indicator brilliant cresyl blue.