Thin films of (Tl,Pb)Sr2Ca0.8Y0.2Cu2O7, and (Tl,Pb)Sr2CuO5 can be grow
n in a single step process which involves sputter deposition from a mi
xed oxide target and simultaneous thermal evaporation of Tl2O. The use
of a radiant heater has allowed extension of this in situ deposition
process to full LaAlO3 and NdGaO3 wafers. Variations in the compositio
n of the deposited film is < 4% across a 50 mm wafer while the thickne
ss uniformity is approximate to 8%. The highest transition temperature
for a (Tl,Pb)Sr2Ca0.8Y0.2Cu2O7 film thus far is 83 K. The RMS surface
roughness of (Tl,Pb)Sr2CuO5 films is uniform across the wafer and app
roximately 1% of the film thickness for films 20 to 100 nm thick.