Yx. Zhang et al., AN INVESTIGATION OF HOMOGENEITY WITHIN MICRO-AREAS OF IAEA URBAN DUSTREFERENCE MATERIALS BY THE SCANNING PROTON MICROPROBE TECHNIQUE, Fresenius' journal of analytical chemistry, 360(3-4), 1998, pp. 356-358
In order to develop new reference materials for microanalytical nuclea
r techniques, the Scanning Proton Microprobe (SPM) technique was used
to determine homogeneity levels within 100 x 200 mu m(2) areas on smal
l pieces of ILEA Urban Dust reference materials. The experimental meth
ods are described in detail. The results show that IAEA-396A/M Vienna
Urban Dust is homogeneous enough for an SRM (less than or equal to 10%
for Si, S, K, Ca, Fe, Cu, Zn) for small sample analysis.