DEVELOPMENT OF POROUS AND DISPERSED CRM

Porous and finely dispersed certified reference materials (CRM) were c ertified using the gas adsorption method. The special certification pr ocedure for IUPAC isotherm classification types I, IT, and IV is prese nted for meso- and macroporous materials with special emphasis on spec ific surface area, specific pore volume and pore width according to st andards DIN 66 131, 66 134, and 66 135. Four CRMs (SiO2, alpha-Al2O3, two transition aluminas) with a macro-and mesopore range are presented . Certification was made on the basis of BCR guidelines in connection with interlaboratory tests (altogether 38 participating laboratories, 44 various gas adsorption apparatus).