Iv. Zarutskii et al., HIGH-TEMPERATURE ELECTROCHEMICAL SYNTHESIS OF TITANIUM DIBORIDE IN HALIDE MELTS, Russian journal of applied chemistry, 70(9), 1997, pp. 1404-1410
The conditions of simultaneous electrolytic reduction of titanium and
boron complexes, composition, form, and the mechanism of formation and
discharge of electrochemically active particles in high-temperature e
lectrochemical synthesis of titanium diboride were studied.