Bf. Sorensen et al., FRACTURE-RESISTANCE MEASUREMENT METHOD FOR IN-SITU OBSERVATION OF CRACK MECHANISMS, Journal of the American Ceramic Society, 81(3), 1998, pp. 661-669
A special test fixture has been developed for fracture mechanical test
ing of brittle materials inside an environmental scanning electron mic
roscope. The fixture loads a double cantilever beam specimen with pure
bending moments and provides stable crack growth. Crack growth is det
ected by in situ observation and acoustic emission, As an example, cra
ck growth in a cubic-phase yttria-stabilized zirconia is detected easi
ly by in situ observation of the crack-tip region, Many fracture tough
ness measurements are obtained for each specimen, giving high confiden
ce in the measured fracture toughness value, In situ observation is us
eful for the study of toughening mechanisms and subcritical crack-grow
th behavior and to sort out erroneous measurements (e.g., due to crack
branching).