N. Kondo et al., STRENGTHENING AND TOUGHENING OF SILICON-NITRIDE BY SUPERPLASTIC DEFORMATION, Journal of the American Ceramic Society, 81(3), 1998, pp. 713-716
Mechanical properties of silicon nitride which was superplastically de
formed in plane-strain compression were investigated. Superplastically
deformed silicon nitride exhibited a highly anisotropic microstructur
e, where rod-shaped grains tended to be aligned along the extruding di
rection. The bending strength and fracture toughness were increased su
bstantially by the deformation process when a stress was applied in th
e extruding direction. It appears that these improvements were mainly
due to effective operation of grain bridging and pull-out by the grain
alignment.