U. Geyer et al., INTERNAL INTERFACES AND INTRINSIC STRESS IN THIN AMORPHOUS CU-TI AND CO-TB FILMS, Journal of applied physics, 83(6), 1998, pp. 3065-3070
A combined investigation of intrinsic stress formation by irt situ sub
strate curvature measurements and of surface morphology evolution by s
canning tunneling microscopy during the growth of amorphous Cu-Ti and
Co-Tb films is reported. Intrinsic tensile stress and surface morpholo
gy are clearly correlated: all films that show intrinsic tensile stres
s formation in the late growth stages exhibit a cluster-like surface m
orphology and vice versa. Both the magnitude of the intrinsic tensile
stress and the cluster size at the surface depend systematically on th
e reduced substrate temperature during film preparation, This dependen
ce fits Hoffman's model for tensile stress formation in thin films. Th
us, the observed surface clusters are probably the top domes of growth
columns, and the atomic mismatch at the column boundaries gives rise
to tensile stress formation. (C) 1998 American Institute of Physics.