A new mineral standard for K-Ar dating, SORI93 biotite, has been prepa
red from the Sori Granodiorite in Gunma Prefecture, Japan. This is int
ended as a substitute of the existing standard, SORI biotite, which is
well calibrated against international standards. The K2O and radiogen
ic Ar-40 contents for SORI93 biotite have been determined to be 8.16 /- 0.04 (1 sigma) wt % and (25.0 +/- 0.1) x 10(-6) (1 sigma) cm(3)STP/
g, respectively. The calculated K-Ar age is 92.6 +/- 0.6 Ma, which is
about 1 million years older than that of SORI biotite. Chloritization
up to 10% partly occur along cleavages of SORI93 biotite. In order to
certify the homogeneity, K2O contents have been repeatedly analyzed fo
r 100, 50, 20 and 10 mg aliquots. The analytical result of 100 mg SORI
93 biotite shows a relative standard deviation similar to that of SORI
biotite and the geochemical standards, JG-1 and JB-1. The standard de
viations of aliquots less than 100 mg are about twice those of the thr
ee standards. This inhomogeneity may be caused by the presence of part
ially chloritized biotite. It is suggested to use 100 mg to ensure the
homogeneity of subsamples.