M. Yoshida et al., INFLUENCE OF GRAVITY ON THE MICROSTRUCTUR E OF DIRECTIONALLY SOLIDIFIED AL-IN MONOTECTIC ALLOY, Nippon Kinzoku Gakkaishi, 62(1), 1998, pp. 85-91
To investigate the influence of gravity on the microstructure of direc
tionally solidified Al-In monotectic alloy, downward U.D.S.(direction
to gravity) and upward U.D.S.(opposite direction to gravity) was carri
ed out. To realize downward U.D.S., zone-melting method was introduced
in order to eliminate cavity which inevitably appears in front of sol
id/liquid interface in current Bridgman method. A hyper-monotectic all
oy, Al-18.0 mass%In, was used to examine gravitational segregation on
both primary and monotectic L-2(In) phases. (1) The gravitational macr
o-segregation and their condensation of primary L-2 liquid were observ
ed at the bottom of molten alloy in the downward U.D.S. In the case of
the upward U.D.S., the primaries dispersed in aligned monotectic morp
hology. On the monotectic reaction, macro-segregation of L-2 liquid gr
owing cooperatively with alpha(Al) phase was not observed neither in u
pward nor in downward U.D.S. However, the morphology in downward U.D.S
. had a tendency to form so called ''banded structure''. (2) In-rich l
ayer with the length of several hundred mu m was found in front of sol
id/liquid interface. The length of In-rich layer in downward U.D.S. wa
s twice longer than in upward U.D.S. in each 6 level growth rate, 1 si
milar to 32 mm/h. (3) Influence of growth rate to the interphase spaci
ng between fibrous monotectic In phases reveal no remarkable differenc
e between upward and downward U.D.S.