FeCo-Cu granular films were prepared by DC magnetron sputtering using
mixed targets. Two kinds of annealing procedures named 'isochronous an
nealing' and 'cumulative isothermal annealing' were used to promote th
e grain growth or phase segregation of as-deposited films. The influen
ce of annealing condition on magnetoresistance has been investigated s
ystematically for the films with optimal composition. It is found that
for the films with same composition, the cumulative isothermal anneal
ed samples have larger giant magnetoresistance (GMR) in comparison wit
h the isochronous annealed ones. Transmission Electron Microscope stud
y shows that the isochronous annealing promotes the grain growth a lit
tle excessively sometimes which is not in favor of the GMR improvement
. The shea-time isothermal annealing at a modest higher temperature, h
owever, limits the grain growth due to the very short annealing time.
By repeating this annealing step several times, more and homogenous fi
ne particles are obtained, which leads to the larger GMR. Therefore, a
cumulative isothermal annealing at an optimal temperature is recommen
ded. (C) 1997 Elsevier Science S.A.