H. Garmestani et al., CHARACTERIZATION OF AL-8090 SUPERPLASTIC MATERIALS USING ORIENTATION IMAGING MICROSCOPY, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 242(1-2), 1998, pp. 284-291
A fundamental understanding of the deformation mechanisms of superplas
ticity requires a detailed characterization of the microstructure. For
certain studies, optical microscopy, transmission electron microscopy
(TEM) and scanning electron microscopy (SEM) techniques used in conve
ntional mode may be inadequate for detailed analysis. This paper prese
nts the use of a newly developed technique, 'orientation imaging micro
scopy' (OIM) in characterizing the microstructure of an Al-8090 alloy
deformed in uniaxial tension to strains of 15, 70 and 660% at 520 degr
ees C and 5 x 10(-4) s(-1) strain rate. In OIM the microstructure is c
onstructed from the measured crystal orientations obtained from points
on the specimen surface distributed in a hexagonal grid, Neighboring
measurements with a misorientation greater than a specified value. ome
ga, misorientation angle criteria (designated by the researcher) are d
eemed to define the location uf grain boundaries. These boundary lines
can be interpreted as high angle grain boundaries or subgrain boundar
ies depending on the value of omega. The implications of the analyses
on superplastic deformation are discussed. (C) 1998 Elsevier Science.