Sc. Liu et al., A STUDY ON FRACTOGRAPHY IN THE LOW-TEMPERATURE BRITTLE-FRACTURE OF AN18CR-18MN-0.7N AUSTENITIC STEEL, Metallurgical and materials transactions. A, Physical metallurgy andmaterials science, 29(3), 1998, pp. 791-798
The fracture mode and crack propagation behavior of brittle fracture a
t 77 and 4 K in an 18Cr-18Mn-0.7N austenitic stainless steel were inve
stigated using optical and scanning electron microscopy. The fracture
path was examined by observing the side surface in a partially rupture
d specimen. The relationship of the fracture facets to the microstruct
ures was established by observing the fracture surface and the adjacen
t side surface simultaneously. Three kinds of fracture facets were ide
ntified at either temperature. The first is a smoothly curved intergra
nular fracture facet with characteristic parallel lines on it. The sec
ond is a fairly planar facet formed by parting along an annealing twin
boundary, a real {111} plane. There are three sets of parallel lines
on the facet and the lines in different sets intersect at 60 deg. The
third is a lamellar transgranular fracture facet with sets of parallel
steps on it. Fracture propagated by the formation of microcracks on a
grain boundary, annealing twin boundary, and coalescence of these cra
cks. The observation suggests that the ease of crack initiation and pr
opagation along the grain boundary and the annealing twin boundary may
be the main reason for the low-temperature brittleness of this steel.
A mechanism for grain boundary cracking, including annealing twin bou
ndary parting, has been discussed based on the stress concentration in
duced by impinging planar deformation structures on the grain boundari
es.