S. Ferrasse et al., DEVELOPMENT OF A SUBMICROMETER-GRAINED MICROSTRUCTURE IN ALUMINUM-6061 USING EQUAL CHANNEL ANGULAR EXTRUSION, Journal of materials research, 12(5), 1997, pp. 1253-1261
Submicrometer-grained (SMG) microstructures are produced in an Al-Mg-S
i alloy (6061) by subjecting peak-aged and overaged billets of the all
oy to intense plastic strain by a process known as equal channel angul
ar extrusion. Two types of refined structure are distinguished by opti
cal and transmission electron microscopy. One structure is created thr
ough intense deformation (four extrusion passes through a 90 degrees d
ie, epsilon = 4.62) by dynamic rotational recrystallization and is a w
ell-formed grain (fragmented) structure with a mean fragment or grain
size of 0.2-0.4 mu m. The other structure is produced by post-extrusio
n annealing through static migration recrystallization, resulting in a
grain size of 5-15 mu m. Intense deformation bf peak-aged material to
a true strain epsilon of 4.62 (four passes) produces a strong, ductil
e, uniform, fine, and high angle grain boundary microstructure with in
creased stability against static recrystallization as compared to the
overaged material.