N. Vivas et al., DEVELOPMENT OF AN ANALYTICAL METHOD FOR T HE DETECTION OF SPECIFIC BIOMARKERS OF WINES AGING IN BARRELS, Analusis, 26(2), 1998, pp. 88-92
Proceeding with a similar way as previous works, we characterised the
presence of lignins in wines. This natural polymer was chosen as bioma
rker. It's a remarkably stable in time and typical wood component. We
used the thioacidolysis reaction with ethanethiol and boron trifluoroe
therate as reagents, to obtain some characteristic phenylpropane units
from the lignin polymer. Identification was performed bq mass spectro
metry coupled with gas chromatography (GPG/SM) of thioacidolysis produ
cts in trimethylsililated form. The aim of this study is the demonstra
tion of wine aging in barrel before bottling.