P. Henner et al., PIPETTE PASTEUR EXTRACTION - A FAST, CONVENIENT, EXHAUSTIVE AND ENVIRONMENTALLY FRIENDLY METHOD FOR THE EXTRACTION OF SOLID SAMPLES, Analusis, 25(9-10), 1997, pp. 51-52
A simple and fast (similar to 5 min) method has been set up to extract
small soil samples (similar to 300 mg) by elution of a small volume o
f methylene chloride (2 000 mu l) on a modified Pasteur pipette. Paste
ur pipette extraction thus allows us to minimize sample losses by evap
oration, degradation, contamination, and experimental handling. Moreov
er, shake and ultrasonic extractions were found to give lower extract
yields, amounting respectively to 1.8 and 1.9 mg.g(-1) dry weight, tha
n pipette Pasteur extraction (3.0 mg.g(-1)). This method may be applie
d to extract the soluble organic matter of any kind of solid sample su
ch as sedimentary rocks, coals aerosols, food and biological substance
s; prior molecular analyses such as gas chromatography coupled to mass
spectrometry.