G. Oskam et Pc. Searson, SOL-GEL SYNTHESIS AND CHARACTERIZATION OF CARBON CERAMIC COMPOSITE ELECTRODES/, JOURNAL OF PHYSICAL CHEMISTRY B, 102(14), 1998, pp. 2464-2468
We have fabricated carbon/ceramic composite electrodes with an interco
nnected network of carbon particles in a silica-based gel. The resulti
ng electrodes were porous and electrically conductive and exhibited ex
cellent stability. BET adsorption measurements combined with electroch
emical techniques such as cyclic voltammetry and electrochemical imped
ance spectroscopy showed that 50% of the carbon surface Nea was access
ible electrochemically.