Hk. Liu et al., PRESSURE INFILTRATION OF SOL GEL PROCESSED SHORT-FIBER CERAMIC-MATRIXCOMPOSITES/, Journal of Materials Science, 33(8), 1998, pp. 2095-2101
Using pressure infiltration short fibre-reinforced ceramic matrix comp
osites with uniform and dense microstructure can be made. Based upon t
his processing technique, composites composed of silica sol, alumina p
articles, and alumina short fibres were fabricated. The related proces
sing parameters studied in this work include infiltration rate, fibre
volume fraction V-f, particle size, and infiltrate viscosity. An optim
al infiltration rate was 4 mm min(-1), at which rate the composite wit
h V-f of 8.1% and particle size of 3 mu m has the highest green densit
y. An equilibrium between particle packing strength and applied load m
ust be obtained during the infiltration to obtain high green density a
nd composite strength. The influence of fibre volume fraction and part
icle size on composite green density is in a synergistic manner becaus
e it involves particle-fibre interactions, fibre-fibre interactions, a
nd sedimentation. Furthermore, the increase of sol viscosity results i
n more sedimentation in the infiltrate and lower composite green densi
ty. The fracture toughness of composites is 38% higher than that of mo
nolithic alumina. (C) 1998 Chapman & Hall.