M. Gonzalez et al., A CONVENIENT ONE-STEP SYNTHESIS OF FORMYLTETRATHIAFULVALENE VINYLOGS - BUILDING-BLOCKS FOR NEW NLO MATERIALS, Tetrahedron letters, 39(20), 1998, pp. 3269-3272
A new method for the synthesis of formyltetrathiafulvalene vinylogs in
which tetrathiafulvalene (TTF) or a substituted derivative of TTF is
metalated with lithium diisopropylamide and then reacted with a vinylo
gous amide to yield the corresponding short polyenals in a one-pot pro
cess is described. (C) 1998 Elsevier Science Ltd. All rights reserved.