A FURTHER 2-LAMBDA(5),4-LAMBDA(5)-DIPHOSP HAPYRIDINE - -AMINO-1-AZA-2-LAMBDA(5),4-LAMBDA(5)-DIPHOSPHININE

Authors
HECKMANN G JONAS E FLUCK E NEUMULLER B
Citation
G. Heckmann et al., A FURTHER 2-LAMBDA(5),4-LAMBDA(5)-DIPHOSP HAPYRIDINE - -AMINO-1-AZA-2-LAMBDA(5),4-LAMBDA(5)-DIPHOSPHININE, Zeitschrift fur Naturforschung. B, A journal of chemical sciences, 53(4), 1998, pp. 443-447
Citations number
24
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
Journal title
Zeitschrift fur Naturforschung. B, A journal of chemical sciences → ACNP
ISSN journal
09320776
Volume
53
Issue
4
Year of publication
1998
Pages
443 - 447
Database
ISI
SICI code
0932-0776(1998)53:4<443:AF2H-->2.0.ZU;2-B
Abstract
2,2,4,4-Tetrakis-(dimethylamino)-6-amino-1-aza-2 lambda(5),4 lambda(5) -diphosphinine (3) has been prepared by reacting 1,1,3,3-tetrakis(dime thylamino)-1 lambda(5)-3 lambda(5)-diphosphete (1) with bis(trimethyls ilyl)carbodiimide (2) in a 2 : 1 molar ratio. Properties, H-1, P-31, a nd C-13 NMR, mass, and IR spectra are reported and discussed. Compound 3 is further characterized by X-ray structure analysis.