T. Krauter et B. Neumuller, THE CRYSTAL-STRUCTURES OF MESSN(CL)ME-2 A ND MES(2)SNCL(2), Zeitschrift fur Naturforschung. B, A journal of chemical sciences, 53(4), 1998, pp. 503-505
Single crystals of MesSn(Cl)Me-2 (1) and Mes(2)SnCl(2) (2) were obtain
ed by the reactions of MesGaCl(2) with Me3SnF and Mes(3)SnF, respectiv
ely. 1 and 2 are monomeric molecules in the solid state. 1: space grou
p P2(1)/n, Z = 4, lattice dimensions at -70 degrees C: a = 1202,3(1),
b = 739,1(1), c = 1441,3(1) pm, beta-102,71(1)degrees, R-1 = 0,0469; 2
: space group Pbcn, Z = 4, lattice dimensions at -50 degrees C: a = 11
07,0(2), b = 949,9(1), c = 1729,8(2) pm, R-1 = 0,049.