X-RAY-INTERFEROMETRIC DETERMINATION OF ANGSTROM-SCALE LATTICE SHIFTS AT THE SURFACE OF SILICON-CRYSTALS - THE ANALOG TO LIGHT-OPTICAL INTERFERENCE MICROSCOPY
M. Bartscher et U. Bonse, X-RAY-INTERFEROMETRIC DETERMINATION OF ANGSTROM-SCALE LATTICE SHIFTS AT THE SURFACE OF SILICON-CRYSTALS - THE ANALOG TO LIGHT-OPTICAL INTERFERENCE MICROSCOPY, Crystal research and technology, 33(4), 1998, pp. 535-541
The paper presents a new imaging method based on a refined and better
stabilised X-ray Michelson interferometer [APPEL, BONSE]. Interference
fringes are detected which mark local Angstrom-scale shifts of the la
ttice at the surface of the interferometer's phase-shifter crystal. Co
nventional double-crystal topography (DCT), lacking phase information
of the beam reflected by the specimen crystal, does not detect mere la
ttice shifts. The new method appears to be also more sensitive to any
combined lattice strain delta = Delta d/d + cot theta(B) Delta theta (
theta(B): Bragg angle, d: lattice parameter) present in the crystal la
yer contributing to the surface Bragg reflection. delta is known to be
the dominant part of the DCT image [BONSE, 1958; BONSE, HARTMANN]. Th
e technique presented here is the X-ray analogue to the well known lig
ht-optical interference microscope. A possible application is the test
ing of silicon crystals for minute lattice imperfections causing latti
ce-incoherent positions of atoms in a surface layer of typical 1 to 10
mu m thickness. For instance striations, which under certain conditio
ns arise during crystal growth, cause such incoherence.