By measuring the polarization of neutrons transmitted through a USb si
ngle crystal we have discovered evidence for a second phase transition
at T = 142(2) K, about 70 K below TN ( = 213 K), in this well-studie
d antiferromagnetic actinide compound. The measurements show that a be
am of polarized neutrons abruptly starts to become depolarized at T.
A number of other measurements find anomalies at T and we propose tha
t the transition is related to dephasing between the components of the
triple-k structure known to exist in USb. This dynamic effect causes
the formation of fluctuating domain walls containing ferromagnetic com
ponents, which then depolarize neutrons.